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Article
Thermal and Optical Properties of CdS Nanoparticles in
Thermotropic Liquid Crystal Monomers
Hooi Ling Lee 1,*, Issam Ahmed Mohammed 2,*, Mohammed Belmahi 3,*, Mohamed Badreddine
Assouar 3, Hervé Rinnert 3 and Marc Alnot 3
1 Nanoscience Research Laboratory, School of Chemical Sciences, University Sains Malaysia, 11800
Penang, Malaysia
2 School of Industrial Technology, University Sains Malaysia, 11800 Penang, Malaysia
3 Institut Jean Lamour, UMR 7198 CNRS, Nancy Université, Université P. Verlaine Metz, Faculté
des Sciences et Techniques B.P. 239 F-54506 Vandoeuvre les Nancy Cedex, France;
E-Mails: badreddine.assouar@lpmi.uhp-nancy.fr (M.B.A.); herve.rinnert@lpm.u-nancy.fr (H.R.);
marc.alnot@lpm.u-nancy.fr (M.A.)
* Author to whom correspondence should be addressed; E-Mails: hooiling78@gmail.com (H.L.L);
issam@usm.my (I.A.M); mohammed.belmahi@lpmi.uhp-nancy.fr (M.B.); Tel.: + 33 383 68 49 24;
Fax: + 33-383-273498.
Received: 10 December 2009; in revised form: 15 February 2010 / Accepted: 17 March 2010 /
Published: 19 March 2010
Abstract: Two new mesogenic monomers, namely 3,3’-dimethoxy-4,4’-
di(hydroxyhexoxy)-N-benzylidene-o-Tolidine (Ia) and 4,4’-di(6-hydroxyhexoxy)-Nbenzylidene-
o-Tolidine (IIa), were reacted with cadmium sulfide (CdS) via an in situ
chemical precipitation method in ethanol to produce CdS nanocomposites. A series of
different mass compositions of CdS with Ia and IIa ranging from 0.1:1.0 to 1.0:1.0 (w/w)
were prepared and characterized using X-ray Diffraction (XRD), Raman spectroscopy,

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